Normall way to calibrate ESC is
- Battery not connected
- Max out servo slider
- Battery connected
- Wait for beeps
- Down servo sliders to minimum
- Wait for final beeps
- Disconnect battery
This is exactly what ESC calibration wizard asks user to do. Check if you followed these steps. If you did that and it still does not work, provide some more information about firmware flight controller version, esc protocol used, esc type/brand and what firmware is running on ESC.